RAS Chemistry & Material ScienceФизика и химия стекла Glass Physics and Chemistry

  • ISSN (Print) 0132-6651
  • ISSN (Online) 3034-6134

Sol-Gel Synthesis of Nanosized Powders and Obtaining Ceramic Composites Based on Zircon and Zirconium Oxide

PII
10.31857/S0132665123600188-1
DOI
10.31857/S0132665123600188
Publication type
Status
Published
Authors
Volume/ Edition
Volume 49 / Issue number 5
Pages
522-531
Abstract
Nanosized precursor powders of (1 – x)ZrSiO4‒xZrO(OH)2 are synthesized by the sol-gel method with the separate precipitation of components to obtain (1 – x)ZrSiO4‒xZrO2 ceramic composites. The thermal behavior of precursor powders is studied by differential scanning calorimetry and thermogravimetry (DSC/TG). Ceramic composites with a high level of microhardness are obtained by sintering powders, preliminarily calcined at 850°C, in air in the temperature range 1000‒1300°C. In the future, such ceramic composites can be used as matrices for solidification and isolating high-level waste (HLW).
Keywords
золь-гель синтез керамические композиты (1 – <i>x</i>)ZrSiO<sub>4</sub>‒<i>x</i>ZrO<sub>2</sub> термический анализ микротвердость по Виккерсу
Date of publication
16.09.2025
Year of publication
2025
Number of purchasers
0
Views
5

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